سامية صلاح الدين الصديق الرائس
عضو هيئة تدريس قار
المؤهل العلمي: ماجستير
الدرجة العلمية: محاضر
التخصص: كيمياء غير عضوية - كيمياء
الكيمياء - العلوم غريان
المنشورات العلمية
pH Role in Green Synthesis of Silver Nanoparticles Using Extract of various Plant Parts: A review
Journal ArticleSynthesizing silver nanoparticles (AgNPs) from extracts of various plant parts
and of agricultural waste is strongly affected by pH. These green synthesis
methods cconsidered simple, cost effective, ecofriendly, and biologically
effective. This brief review aimed to survey the role of pH in the green
synthesis of AgNPs using those media, with a focus on its effect on AgNPs
morphology and size. This review article revealed that the alkaline pH (9 -
10) is the optimum condition for synthesizing more stable and tiny uniform
AgNPs. In addition, according to the reviewed articles, the spherical shape is
the most dominant shape of these articles in the basic medium and the size of
these particles decreases at elevated pH values and ranged from 5-40 nm
Abdulnasir Albasheer Alsagagheer Omar, Samia Salahaddin Alseddeq Raies, Mofida Mohamed Rajab Alfaid, Kawther Elbahlool Salem Adaila, (10-2024), ليبيا: Scientific Journal for the Faculty of Science-Sirte University, 4 (2), 101-108
دليل كتابة الورقة البحثية
كتابتعد الأوراق البحثية وسيلة ً مهمة لعرض ما توصل إليه الباحث من نتائج تجاربه العلمية، حيث إن العلم لا يعرف إلا إذا تم تسجيله ونشره للاستفادة منه. ولكي يتم إيصال هذا العلم بكفاءة وفعالية وبكتابة علمية جيدة، جاءت فكرة هذا الكتاب لكي يكون دليلا ً ومرشدا للباحثين المتحدثين باللغة العربية في كتابة بحوثهم وكيفية نشرها. نظرا للنقص الواضح في عدد الكتب العربية التي تعنى بالكتابة والنشر العلمي، صمم هذا الكتاب ليعمل كدليل إرشادي يساعد الباحثين وطالب العلم العرب في كيفية كتابة ونشر بحوثهم، ويقدم شرحا مفصلا عن كل خطوة من خطوات كتابة الورقة البحثية بأجزائها وأنواعها المختلفة ابتداء من العنوان حتى النتائج والمناقشة ...والخ. كما أنه يتناول بعض التوضيحات عن كيفية اختيار المجلة وخطوات النشر.
عبدالناصر البشير الصغير عمر، مفيدة محمد رجب الفيض، سامية صلاح الدين الصديق الرائس، كوثر البهلول سالم اعديلة، (02-2024)، مصر: دار ومكتبة الشعب للطباعة والنشر والتوزيع،
Exploiting pear leaves in biosynthesis of silver nanoparticles
Journal ArticleBiosynthesis techniques have a number of advantages over other methods for producing silver nanoparticles (AgNPs), which provide a wide range of applications. The present work highlights the biosynthesis of AgNPs by mixing pear leaf aqueous extract with silver nitrate, and the formation of AgNPs was observed by the change of mixture color from yellow to dark brown and visible spectrophotometry. Moreover, the effect of pH, reaction time, AgNO3 concentration, extract volume and temperature on the suggested approach was also studied. The results showed that pear leaf aqueous extract is an excellent material for the biosynthesis of AgNPs, and by controlling the mentioned parameters that influence synthesis, a large number of AgNPs with small sizes may be produced. Keywords: silver nitrate, silver nanoparticles, pear leaves, biosynthesis
Nawal Abdurazq Elhadi Ahmad, Samia Salahaddin Alseddeq Raies, Kawther Elbahlool Salem Adaila, Abdounasser Albasher Omar, (06-2023), online: LJAST, 1 (-1), -1--3
Exploiting Pear Leaves In Biosynthesis Of Silver Nanoparticles
Journal ArticleBiosynthesis techniques have a number of advantages over other methods for producing silver nanoparticles (AgNPs), which provide a wide range of applications. The present work highlights the biosynthesis of AgNPs by mixing pear leaf aqueous extract with silver nitrate, and the formation of AgNPs was observed by the change of mixture color from yellow to dark brown and visible spectrophotometry. Moreover, the effect of pH, reaction time, AgNO3 concentration, extract volume and temperature on the suggested approach was also studied. The results showed that pear leaf aqueous extract is an excellent material for the biosynthesis of AgNPs, and by controlling the mentioned parameters that influence synthesis, a large number of AgNPs with small sizes may be produced.
Abdulnasir Albasheer Alsagagheer Omar, Nawal Abdurazq Elhadi Ahmad, Samia Salahaddin Alseddeq Raies, Kawther Elbahlool Salem Adaila, (06-2023), ليبيا: مجلة لیبیا للعلوم التطبیقیة والتقنیة, 11 (1), 1-10
Aqueous Extract of Winter Jasmine Leaves Mediated Biosynthesis of Silver Nanoparticles
Journal ArticleThis study reports a rapid and eco-friendly green method for the synthesis of silver nanoparticles from silver nitrate solution using winter jasmine leaves extract as a reducing agent of Ag+ to Ag0. A visible Absorption Spectrophotometer was used to monitor the formation of silver nanoparticles (AgNPs). The visible spectrum showed an absorption peak at 420 nm which reflects the surface plasmon resonance (SPR) of AgNPs. In addition to that, the synthesis of AgNPs was confirmed by the color change of the solution. By studying the most important factors affecting the formation of AgNPs, it was noted that the productivity of AgNPs in the solution increased by increasing the pH of the solution, and the basic medium was the appropriate medium for the synthesis process. Also, the amount of produced AgNPs increased with the increase in temperature, volume of extract, reaction time, the extract volume ratio of the winter jasmine leaves, and silver nitrate concentration. In conclusion, the aqueous extract of winter jasmine leaves represents a suitable material for the biosynthesis of AgNPs, and large amounts of AgNPs with appropriate sizes may be obtained by controlling the parameters that affect the synthesis process.
Abdulnasir Albasheer Alsagagheer Omar, Kawther Elbahlool Salem Adaila, Samia Salahaddin Alseddeq Raies, (04-2023), ليبيا: Scientific Journal for the Faculty of Science-Sirte University, 3 (1), 95-101